C₁₇H₂₄O₄S

Base Information

• Chemical Name: C₁₇H₂₄O₄S
• CAS No.: 1404197-52-9
• Molecular Formula: C₁₇H₂₄O₄S
• Molecular Weight: 324.441
• Mol file: 1404197-52-9.mol

Synonyms:C₁₇H₂₄O₄S

Chemical Property of C₁₇H₂₄O₄S

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of C₁₇H₂₄O₄S

There total 1 articles about C₁₇H₂₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C10H18O2 (1404197-51-8) + p-toluenesulfonyl chloride (98-59-9) → C17H24O4S (1404197-52-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol3026395

Reference yield: 95.0%

C17H24O4S (1404197-52-9) → C10H17N3O (1404197-53-0)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 90 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol3026395

Reference yield:

C17H24O4S (1404197-52-9) → C10H17NO + C10H17NO

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere

3: triphenylphosphine / tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere

With sodium azide; triphenylphosphine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 3: |Staudinger Azide Reduction;

DOI:10.1021/ol3026395

upstream raw materials:

C₁₀H₁₈O₂

p-toluenesulfonyl chloride

Downstream raw materials:

C₁₀H₁₇N₃O