methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside

Base Information

Chemical Name:methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside
CAS No.:174278-22-9
Molecular Formula:C₁₇H₂₄O₇S
Molecular Weight:372.439
Hs Code.:

Synonyms:methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside

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Chemical Property of methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside

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Technology Process of methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside

There total 2 articles about methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 174278-21-8
Imidazole-1-carbothioic acid O-[(3aS,4S,6R,7R,7aS)-4-methoxy-2,2-dimethyl-6-(toluene-4-sulfonyloxymethyl)-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl] ester

: 174278-22-9
methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside

Guidance literature:: With tri-n-butyl-tin hydride; In toluene; for 3h; Heating;
DOI:10.1016/0008-6215(95)00324-X

Reference yield:

: 112612-45-0
methyl 2,3-O-isopropylidene-6-O-p-toluenesulfonyl-α-D-mannopyranoside

: 174278-22-9
methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 69.2 percent / toluene / 4 h / Heating

2: 84.3 percent / Bu₃SnH / toluene / 3 h / Heating

With tri-n-butyl-tin hydride; In toluene;
DOI:10.1016/0008-6215(95)00324-X

Reference yield:

: 174278-22-9
methyl 4-deoxy-2,3-O-isoprpylidene-6-O-(p-tolylsulfonyl)-α-D-lyxo-hexopyranoside

: 1279230-33-9
4,6-dideoxy-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / sodium amalgam, H₂O / methanol / 12 h / Ambient temperature

2: 70.8 percent / sodium borohydride / dimethylsulfoxide / 2 h / 80 °C

3: Amberlit IR-120 (H⁺ form), water / 16 h / Heating

With sodium tetrahydroborate; sodium amalgam; Amberlit IR-120 (H⁺ form); water; In methanol; dimethyl sulfoxide;
DOI:10.1016/0008-6215(95)00324-X