2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid

Base Information

Chemical Name:2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid
CAS No.:79622-69-8
Molecular Formula:C₁₇H₂₅NO₄
Molecular Weight:308.382
Hs Code.:

2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten<sup>(1)</sup>yl)-N,N-diethyl-benzoesaeureamid

Synonyms:2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid

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Chemical Property of 2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid

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Technology Process of 2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid

There total 4 articles about 2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 79622-67-6
2,3-Dimethoxy-6-(buten⁽¹⁾-on⁽³⁾yl)-N,N-diethyl-benzoesaeureamid

: 79622-69-8
2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid

Guidance literature:: With sodium borodeuteride; In methanol; Ambient temperature;
DOI:10.1002/ardp.19813140805

Reference yield:

: 79622-66-5
1-Chlor-4,5-dimethoxy-isobenzofuran-3-on

: 79622-69-8
2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 2 h / Heating

2: 54 percent / aq. NaOH / methanol; acetone / 18 h / Ambient temperature

3: 84 percent / NaB⁽²⁾H₄ / methanol / Ambient temperature

With sodium hydroxide; sodium borodeuteride; In methanol; chloroform; acetone;
DOI:10.1002/ardp.19813140805

Reference yield:

: 519-05-1
opianic acid

: 79622-69-8
2,3-Dimethoxy-6-(3'-deutero-3'-hydroxybuten⁽¹⁾yl)-N,N-diethyl-benzoesaeureamid

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / CHCl₃ / 3 h / Heating

2: CHCl₃ / 2 h / Heating

3: 54 percent / aq. NaOH / methanol; acetone / 18 h / Ambient temperature

4: 84 percent / NaB⁽²⁾H₄ / methanol / Ambient temperature

With sodium hydroxide; thionyl chloride; sodium borodeuteride; In methanol; chloroform; acetone;
DOI:10.1002/ardp.19813140805