Technology Process of C23H32N2O2
There total 3 articles about C23H32N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-Methyl-propane-2-sulfinic acid ((1R,2R)-2-benzylamino-3-methyl-1-phenyl-butyl)-amide;
With
hydrogenchloride;
In
1,4-dioxane; methanol;
at 20 ℃;
for 0.5h;
Inert atmosphere;
di-tert-butyl dicarbonate;
With
triethylamine;
In
dichloromethane;
Inert atmosphere;
DOI:10.1002/ejoc.201100299
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: samarium diiodide; tert-butyl alcohol / tetrahydrofuran / -78 °C / Inert atmosphere
2.1: copper diacetate; acetic acid; zinc / water / 1 h / 70 °C / Inert atmosphere
3.1: hydrogenchloride / 1,4-dioxane; methanol / 0.5 h / 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
hydrogenchloride; samarium diiodide; copper diacetate; acetic acid; zinc; tert-butyl alcohol;
In
tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1002/ejoc.201100299
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: samarium diiodide; tert-butyl alcohol / tetrahydrofuran / -78 °C / Inert atmosphere
2.1: copper diacetate; acetic acid; zinc / water / 1 h / 70 °C / Inert atmosphere
3.1: hydrogenchloride / 1,4-dioxane; methanol / 0.5 h / 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
hydrogenchloride; samarium diiodide; copper diacetate; acetic acid; zinc; tert-butyl alcohol;
In
tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1002/ejoc.201100299
