tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

Base Information

Chemical Name:tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate
CAS No.:84247-41-6
Molecular Formula:CH₂O₃*2C₄₃H₆₅N₇O₂₀
Molecular Weight:2062.07
Hs Code.:

Synonyms:tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

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Chemical Property of tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

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Technology Process of tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

There total 1 articles about tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 84247-39-2
tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-2''-N-(benzyloxycarbonyl)-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin

: 84247-41-6
tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

Guidance literature:: With hydrogen; palladium; In ethanol; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(82)84031-7

Reference yield: 35.0%

: 84247-41-6
tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

: 84247-43-8
tetra-N(G)-acetyl-2,5,6-tri-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

Guidance literature:: With ethanol; at 28 ℃; for 72h;
DOI:10.1016/0008-6215(82)84031-7

Reference yield:

: 84247-41-6
tetra-N(G)-acetyl-2,5,6,3''-tetra-O-acetyl-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin carbonate

: 89113-24-6
tetra-N(G)-acetyl-2,5,6-tri-O-acetyl-2''-N-(benzyloxycarbonyl)-3''-O-(trifluoromethylsulfonyl)-3',3'a:4'',6''-di-O-isopropylidenedihydrostreptomycin

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / EtOH / 72 h / 28 °C

2: 98 percent / 0.7percent aq. NaHCO₃ / CHCl₃ / 1 h / Ambient temperature

3: CH₂Cl₂; pyridine / 8 h / 5 °C

With ethanol; sodium hydrogencarbonate; In pyridine; dichloromethane; chloroform;
DOI:10.1016/0008-6215(82)84031-7