C.I. Disperse yellow 64

Base Information

• Chemical Name: C.I. Disperse yellow 64
• CAS No.: 10319-14-9
• Deprecated CAS: 12223-86-8,66565-57-9
• Molecular Formula: C18H10BrNO3
• Molecular Weight: 368.186
• Hs Code.: 2933499090
• European Community (EC) Number: 233-701-7
• DSSTox Substance ID: DTXSID2044503
• Nikkaji Number: J236.764E
• Wikidata: Q72469933
• ChEMBL ID: CHEMBL3185278
• Mol file: 10319-14-9.mol

Synonyms:Disperse Yellow 64;10319-14-9;C.I. DISPERSE YELLOW 64;disperse yellow 3g;12223-86-8;2-(4-bromo-3-hydroxyquinolin-2-yl)indene-1,3-dione;1H-Indene-1,3(2H)-dione, 2-(4-bromo-3-hydroxy-2-quinolinyl)-;DTXSID2044503;EINECS 233-701-7;C.I. Disperse yellow 64;4-Bromo-3-hydroxy-2-(1,3-indandion-2-yl)quinoline;2-(4-Bromo-3-hydroxy-2-quinolyl)-1H-indene-1,3(2H)-dione;C.I.Solvent yellow 176;C18H10BrNO3;Solvent Yellow 176;SCHEMBL2391662;CHEMBL3185278;DTXCID0024503;C18-H10-Br-N-O3;Tox21_300734;MFCD00071862;AKOS015913859;NCGC00248154-01;NCGC00254640-01;CAS-10319-14-9;DISPERSE YELLOW 64 (LATYL YELLOW 3 GB);W-110267;2-(4-bromo-3-hydroxyquinolin-2-yl)-1H-indene-1,3(2H)-dione

Chemical Property of C.I. Disperse yellow 64

Chemical Property:

• Appearance/Colour: Deep orange powder
• Melting Point: 242-244 °C
• Boiling Point: 505.4 °C at 760 mmHg
• PKA: -3.33±0.20(Predicted)
• Flash Point: 259.5 °C
• PSA: 67.26000
• Density: 1.691 g/cm³
• LogP: 3.86570
• Storage Temp.: Amber Vial, -20°C Freezer
• Solubility.: Aqueous Base (Slightly), DMSO (Slightly), Methanol (Slightly), Water (Slightly,
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 366.98441
• Heavy Atom Count: 23
• Complexity: 487

Purity/Quality:

98%min ^*data from raw suppliers

DisperseYellow64(TechnicalGrade) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)C(C2=O)C3=NC4=CC=CC=C4C(=C3O)Br
• Uses: Disperse Yellow 64, tech. (CAS# 10319-14-9) is used in the short-process dyeing and finishing process of polyester/nylon viscose fabric.

Technology Process of C.I. Disperse yellow 64

There total 2 articles about C.I. Disperse yellow 64 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

2-(3-hydroxy-2-quinolinyl)-1H-indene-1,3(2H)-dione (7576-65-0,113041-80-8,12223-85-7,62395-98-6) → 2-(4-bromo-3-hydroxy-2-quinolinyl)indan-1,3-dione (10319-14-9)

Guidance literature:

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; In dichloromethane; at 40 ℃; for 8h; Time;

Reference yield:

→ 2-(4-bromo-3-hydroxy-2-quinolinyl)indan-1,3-dione (10319-14-9)

Guidance literature:

3-Hydroxychinaldin-4-carbonsaeure, Phthalsaeureanhydrid, Brom;

upstream raw materials:

2-(3-hydroxy-2-quinolinyl)-1H-indene-1,3(2H)-dione

Refernces

• 1、 -. "Preparation process of solvent dye". Paragraph 0017; 0019; 0020; 0021. . Retrieved 2018/06/26.