2-(bromomethyl)-9-phenylnonyl bromide

Base Information

Chemical Name:2-(bromomethyl)-9-phenylnonyl bromide
CAS No.:221657-09-6
Molecular Formula:C₁₆H₂₄Br₂
Molecular Weight:376.175
Hs Code.:

Synonyms:2-(bromomethyl)-9-phenylnonyl bromide

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Chemical Property of 2-(bromomethyl)-9-phenylnonyl bromide

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Technology Process of 2-(bromomethyl)-9-phenylnonyl bromide

There total 5 articles about 2-(bromomethyl)-9-phenylnonyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 221657-08-5
2-(hydroxymethyl)-9-phenylnonanol

: 221657-09-6
2-(bromomethyl)-9-phenylnonyl bromide

Guidance literature:: With phosphorus tribromide; In N,N-dimethyl-formamide; 0 deg C to rt;
DOI:10.1021/jo981617q

Reference yield:

: 4549-31-9
1,7-dibromoheptane

: 221657-09-6
2-(bromomethyl)-9-phenylnonyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / tetrahydrofuran; diethyl ether; cyclohexane / -78 deg C to rt

2: 6.63 g / Na / ethanol / 4 h / Heating

3: 40 percent / LiAlH₄ / tetrahydrofuran / 72 h / Heating

4: 77 percent / PBr₃ / dimethylformamide / 0 deg C to rt

With lithium aluminium tetrahydride; sodium; phosphorus tribromide; In tetrahydrofuran; diethyl ether; ethanol; cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/jo981617q

Reference yield:

: 78573-85-0
1-bromo-7-phenyl-heptane

: 221657-09-6
2-(bromomethyl)-9-phenylnonyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 6.63 g / Na / ethanol / 4 h / Heating

2: 40 percent / LiAlH₄ / tetrahydrofuran / 72 h / Heating

3: 77 percent / PBr₃ / dimethylformamide / 0 deg C to rt

With lithium aluminium tetrahydride; sodium; phosphorus tribromide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo981617q