Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone

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Chemical Name:Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone
CAS No.:147089-51-8
Molecular Formula:C₂₅H₂₅NOS₂
Molecular Weight:419.612
Hs Code.:

Synonyms:Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone

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Chemical Property of Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone

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Technology Process of Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone

There total 5 articles about Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 147089-41-6
2-(2-Cyclohexyl-benzo[1,3]oxathiol-2-yl)-4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrole

: 147089-51-8
Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone

Guidance literature:: With tetrafluoroboric acid diethyl ether; In ethanol; for 1h; Ambient temperature;

Reference yield:

: 97188-29-9
1-(phenylsulfonyl)-3-(4-methylbenzoyl)pyrrole

: 147089-51-8
Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / HBF₄-diethyl ether complex / benzene / Heating

2: 100 percent / 10percent aq. KOH / dioxane; methanol / 0.25 h / 50 °C

3: 90 percent / pyridine / acetonitrile / 4 h / Ambient temperature

4: 95 percent / HBF₄-diethyl ether complex / ethanol / 1 h / Ambient temperature

With pyridine; tetrafluoroboric acid diethyl ether; potassium hydroxide; In 1,4-dioxane; methanol; ethanol; acetonitrile; benzene;

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 147089-51-8
Cyclohexyl-[4-(2-p-tolyl-benzo[1,3]dithiol-2-yl)-1H-pyrrol-2-yl]-methanone

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / anhydrous AlCl₃ / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 96 percent / HBF₄-diethyl ether complex / benzene / Heating

3: 100 percent / 10percent aq. KOH / dioxane; methanol / 0.25 h / 50 °C

4: 90 percent / pyridine / acetonitrile / 4 h / Ambient temperature

5: 95 percent / HBF₄-diethyl ether complex / ethanol / 1 h / Ambient temperature

With pyridine; tetrafluoroboric acid diethyl ether; potassium hydroxide; aluminium trichloride; In 1,4-dioxane; methanol; ethanol; dichloromethane; acetonitrile; benzene;