dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Base Information

• Chemical Name: dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside
• CAS No.: 1115586-49-6
• Molecular Formula: C₅₄H₇₃NO₁₂Si
• Molecular Weight: 956.259

Synonyms:dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Chemical Property of dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

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Technology Process of dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

There total 2 articles about dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside (1115586-48-5) → dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside (1115586-49-6)

Guidance literature:

With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1016/j.carres.2008.10.007

Reference yield:

C54H71NO12Si → dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside (1115586-49-6) + dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-mannpyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside (478551-71-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; dichloromethane; at 0 - 20 ℃; for 12h;

DOI:10.1016/j.carres.2008.10.007

Reference yield:

dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside (1115586-49-6) → C54H71NO12Si

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.carres.2008.10.007

upstream raw materials:

dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

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