(C₄H₉)4N⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₄H₉)4N)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)

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Chemical Name:(C₄H₉)4N⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₄H₉)4N)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)
CAS No.:282726-77-6
Molecular Formula:C₁₆H₃₆N*C₁₇H₁₁Cl₃F₁₀N₃W
Molecular Weight:979.956
Hs Code.:

(C<sub>4</sub>H<sub>9</sub>)4N<sup>(1+)</sup>*(CH<sub>3</sub>N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)2)WCl<sub>3</sub><sup>(1-)</sup>=((C<sub>4</sub>H<sub>9</sub>)4N)((CH<sub>3</sub>N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)2)WCl<sub>3</sub>)

Synonyms:(C₄H₉)4N⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₄H₉)4N)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)

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Chemical Property of (C₄H₉)4N⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₄H₉)4N)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)

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Technology Process of (C₄H₉)4N⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₄H₉)4N)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)

There total 1 articles about (C₄H₉)4N⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₄H₉)4N)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 282726-75-4
(C₂H₅)3NH⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₂H₅)3NH)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)

: 1112-67-0
tetrabutyl-ammonium chloride

: 282726-77-6
(C₄H₉)4N⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₄H₉)4N)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)

Guidance literature:: In tetrahydrofuran; byproducts: Et3NHCl; under N2; Bu4NCl (1.2 equiv.) added to soln. of W complex in THF; stirred for 12 h; filtered through Celite; volatiles removed from filtrate in vac.; dissolved in toluene; filtered; vol. of filtrate reduced in vac.; added dropwise to rapidly stirred pentane; ppt. collected on frit; washed with pentane; dried in vac.; elem. anal.;
DOI:10.1021/om030638u