Technology Process of C33H40O8
There total 6 articles about C33H40O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine hydrofluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 2.16667h;
DOI:10.1016/j.tet.2013.12.066
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridinium p-toluenesulfonate / dichloromethane / 1.25 h
2.1: n-butyllithium / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C / Inert atmosphere
2.2: 2.5 h / -78 °C / Inert atmosphere
3.1: potassium carbonate / water / 0.5 h / 0 °C
3.2: 0 - 20 °C
4.1: lithium tert-butoxide / tetrahydrofuran / 0.33 h
4.2: 0.5 h
4.3: 16.5 h
5.1: pyridine hydrofluoride / tetrahydrofuran / 2.17 h / 0 - 20 °C
With
n-butyllithium; pyridine hydrofluoride; pyridinium p-toluenesulfonate; potassium carbonate; lithium tert-butoxide;
In
tetrahydrofuran; dichloromethane; cyclohexane; water;
3.1: |Horner-Wadsworth-Emmons Olefination / 3.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.tet.2013.12.066
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C / Inert atmosphere
1.2: 2.5 h / -78 °C / Inert atmosphere
2.1: potassium carbonate / water / 0.5 h / 0 °C
2.2: 0 - 20 °C
3.1: lithium tert-butoxide / tetrahydrofuran / 0.33 h
3.2: 0.5 h
3.3: 16.5 h
4.1: pyridine hydrofluoride / tetrahydrofuran / 2.17 h / 0 - 20 °C
With
n-butyllithium; pyridine hydrofluoride; potassium carbonate; lithium tert-butoxide;
In
tetrahydrofuran; cyclohexane; water;
2.1: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.tet.2013.12.066
