N,N'-bissulfuric diamide

Base Information

• Chemical Name: N,N'-bissulfuric diamide
• CAS No.: 102989-18-4
• Molecular Formula: C₂₆H₁₆N₆O₁₄S
• Molecular Weight: 668.511

Synonyms:N,N'-bissulfuric diamide

Chemical Property of N,N'-bissulfuric diamide

Chemical Property:

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Technology Process of N,N'-bissulfuric diamide

There total 1 articles about N,N'-bissulfuric diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N,N'-bissulfurous diamide (102989-17-3) → N,N'-bissulfuric diamide (102989-18-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 5 ℃; for 1h;

DOI:10.1055/s-1987-27876

Reference yield: 81.0%

N,N'-bissulfuric diamide (102989-18-4) + ethylenediamine (107-15-3,85404-18-8) → 4-(2-nitrophenoxy)-7,8-dihydro-6H-imidazo<2,1-c><1,2,4,6>thiatriazine 2,2-dioxide (102989-16-2)

Guidance literature:

In acetonitrile; at 20 ℃; for 16h;

DOI:10.1055/s-1987-27876

Reference yield: 75.0%

ethylamine (75-04-7,85404-22-4) + N,N'-bissulfuric diamide (102989-18-4) → 4-Ethyl-3,5-bis-(2-nitro-phenoxy)-4H-[1,2,4,6]thiatriazine 1,1-dioxide (110023-80-8)

Guidance literature:

In acetonitrile; at 20 ℃; for 1h;

DOI:10.1055/s-1987-27876

upstream raw materials:

N,N'-bissulfurous diamide

Downstream raw materials:

4-Ethyl-3,5-bis-(2-nitro-phenoxy)-4H-[1,2,4,6]thiatriazine 1,1-dioxide

4-Isopropyl-3,5-bis-(2-nitro-phenoxy)-4H-[1,2,4,6]thiatriazine 1,1-dioxide

4-(2-nitrophenoxy)-7,8-dihydro-6H-imidazo<2,1-c><1,2,4,6>thiatriazine 2,2-dioxide

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