C₂₉H₃₀N₂O₁₀S

Base Information

Chemical Name:C₂₉H₃₀N₂O₁₀S
CAS No.:1262795-75-4
Molecular Formula:C₂₉H₃₀N₂O₁₀S
Molecular Weight:598.631
Hs Code.:

C<sub>29</sub>H<sub>30</sub>N<sub>2</sub>O<sub>10</sub>S

Synonyms:C₂₉H₃₀N₂O₁₀S

Suppliers and Price of C₂₉H₃₀N₂O₁₀S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₉H₃₀N₂O₁₀S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₉H₃₀N₂O₁₀S

There total 9 articles about C₂₉H₃₀N₂O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1262795-73-2
C₂₆H₂₈N₂O₁₀S

: 106-96-7
propargyl bromide

: 1262795-75-4
C₂₉H₃₀N₂O₁₀S

Guidance literature:: C₂₆H₂₈N₂O₁₀S; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 1.5h; Inert atmosphere;

propargyl bromide; In N,N-dimethyl-formamide; toluene; mineral oil; at 0 - 18 ℃; for 2h; Inert atmosphere;
DOI:10.1071/CH10359

Reference yield:

: C₁₂H₁₆BrNO₃

: 1262795-75-4
C₂₉H₃₀N₂O₁₀S

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,4-dioxane / 24 h / 105 °C

2.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 2 h / 18 °C / Inert atmosphere

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; caesium carbonate / tetrahydrofuran; water / 2 h / 65 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 0 °C / Inert atmosphere

5.2: 2 h / 0 - 18 °C / Inert atmosphere

With 2,6-dimethylpyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; trimethylsilyl trifluoromethanesulfonate; potassium acetate; sodium hydride; caesium carbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 4.1: Suzuki coupling;
DOI:10.1071/CH10359

Reference yield:

: 1027032-85-4
C₁₂H₂₀O₂

: 1262795-75-4
C₂₉H₃₀N₂O₁₀S

Guidance literature:: Multi-step reaction with 8 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 40 °C / Inert atmosphere

2.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / dichloromethane; water / 4 h / 18 °C / Inert atmosphere

3.1: 1,4-dioxane / 18 h / 80 °C

4.1: 1,4-dioxane / 24 h / 105 °C

5.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 2 h / 18 °C / Inert atmosphere

7.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; caesium carbonate / tetrahydrofuran; water / 2 h / 65 °C / Inert atmosphere

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 0 °C / Inert atmosphere

8.2: 2 h / 0 - 18 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; trimethylsilyl trifluoromethanesulfonate; N-benzyl-N,N,N-triethylammonium chloride; potassium acetate; sodium hydride; caesium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 7.1: Suzuki coupling;
DOI:10.1071/CH10359