diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

Base Information

Chemical Name:diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester
CAS No.:406725-48-2
Molecular Formula:C₂₃H₂₈N₃O₅P
Molecular Weight:457.466
Hs Code.:

Synonyms:diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

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Chemical Property of diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

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Technology Process of diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

There total 3 articles about diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 406725-88-0
(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

: 406725-48-2
diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

Guidance literature:: With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1021/ol017240j

Reference yield:

: 5001-26-3
2-hydroxy-N-(benzyl)benzylamine

: 406725-48-2
diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / K₂CO₃ / acetonitrile

2: 85 percent / DCC; DMAP / CH₂Cl₂

3: 62 percent / p-acetamidobenzenesulfonyl azide; DBU / acetonitrile

With dmap; 4-acetamidobenzenesulfonyl azide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/ol017240j

Reference yield:

: 406725-37-9
2-[(allyl-benzyl-amino)-methyl]-phenol

: 406725-48-2
diazo-(diethoxy-phosphoryl)-acetic acid 2-[(allyl-benzyl-amino)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / DCC; DMAP / CH₂Cl₂

2: 62 percent / p-acetamidobenzenesulfonyl azide; DBU / acetonitrile

With dmap; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/ol017240j