C₂H₅C₆H₄C(O)PC(N(CH₃)2)2

Base Information

• Chemical Name: C₂H₅C₆H₄C(O)PC(N(CH₃)2)2
• CAS No.: 1084798-09-3
• Molecular Formula: C₁₄H₂₁N₂OP
• Molecular Weight: 264.307
• Mol file: 1084798-09-3.mol

Synonyms:C₂H₅C₆H₄C(O)PC(N(CH₃)2)2

Chemical Property of C₂H₅C₆H₄C(O)PC(N(CH₃)2)2

Chemical Property:

Purity/Quality:

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Technology Process of C₂H₅C₆H₄C(O)PC(N(CH₃)2)2

There total 1 articles about C₂H₅C₆H₄C(O)PC(N(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

p-ethylbenzoyl chloride (16331-45-6) + (trimethylsilyl)phosphine (83716-84-1) → C2H5C6H4C(O)PC(N(CH3)2)2 (1084798-09-3)

Guidance literature:

In pentane; at -30 ℃; for 1h;

DOI:10.1002/ejic.200700440

Reference yield: 36.0%

C2H5C6H4C(O)PC(N(CH3)2)2 (1084798-09-3) + [(C5H5)Mo(CO)2Cl(PH(C6H5)2)] → [(C5H5)Mo(CO)2(P(C6H5)2OC(P)C6H4C2H5)]

Guidance literature:

With DBU; In toluene; N2, a soln. of metal compd. added at -30°C to a soln. of P compd.(exces) and DBU, stirred for 1 h at -30°C, stirred at 20° C for 12 h; volatiles removed (vac.), evapd. with toluene and Florisil to dryness, chromy. (Florisil, pentane/diethyl ether), concd., stored for 12 h at -30°C; elem. anal.;

DOI:10.1002/ejic.200700440

Reference yield: 30.0%

C2H5C6H4C(O)PC(N(CH3)2)2 (1084798-09-3) + (η(5)-C5H5)W(CO)2ClPHPh2 → [(C5H5)W(CO)2(P(C6H5)2OC(P)C6H4C2H5)]

Guidance literature:

With DBU; In toluene; N2, a soln. of metal compd. added at -10°C to a soln. of P compd.(exces) and DBU, stirred at room. temp. for 12 h; evapd. to dryness, chromy. (Florisil, pentane/diethyl ether), concd., stored for 24 h at -30°C; elem. anal.;

DOI:10.1002/ejic.200700440

upstream raw materials:

p-ethylbenzoyl chloride

(trimethylsilyl)phosphine