Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester
CAS No.:737788-40-8
Molecular Formula:C₇₃H₇₈O₁₂Si
Molecular Weight:1175.5
Hs Code.:

Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

Synonyms:Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

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Chemical Property of Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

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Technology Process of Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

There total 2 articles about Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 150772-61-5
3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-mannopyranose 1,2-(pent-4-enyl orthobenzoate)

: 202845-42-9
1-O-allyl-3,4,5-tri-O-benzyl-D-myo-inositol

: 737788-40-8
Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

Guidance literature:: With N-iodo-succinimide; ytterbium(III) triflate;
DOI:10.1016/j.bmcl.2004.04.103

Reference yield: 26.0%

: 150772-61-5
3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-mannopyranose 1,2-(pent-4-enyl orthobenzoate)

: 202845-42-9
1-O-allyl-3,4,5-tri-O-benzyl-D-myo-inositol

: 737788-40-8
Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

: C₁₁₆H₁₂₂O₁₈Si₂

Guidance literature:: With N-iodo-succinimide; t-butyldimethylsiyl triflate;
DOI:10.1016/j.bmcl.2004.04.103

Reference yield: 42.0%

: ((3aS,5R,6R,7S,7aS)-6,7-Bis-benzyloxy-2-pent-4-enyloxy-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran-5-ylmethoxy)-tert-butyl-dimethyl-silane

: 737788-40-8
Benzoic acid (2R,3S,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-allyloxy-4,5,6-tris-benzyloxy-3-hydroxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-yl ester

: C₁₀₆H₁₁₈O₁₈Si₂

Guidance literature:: With N-iodo-succinimide; scandium tris(trifluoromethanesulfonate); In dichloromethane; for 0.333333h; cooling;
DOI:10.1002/anie.200500505