C₇₀H₈₄O₁₇

Base Information

Chemical Name:C₇₀H₈₄O₁₇
CAS No.:180074-75-3
Molecular Formula:C₇₀H₈₄O₁₇
Molecular Weight:1197.43
Hs Code.:

C<sub>70</sub>H<sub>84</sub>O<sub>17</sub>

Synonyms:C₇₀H₈₄O₁₇

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Chemical Property of C₇₀H₈₄O₁₇

Chemical Property:

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Technology Process of C₇₀H₈₄O₁₇

There total 12 articles about C₇₀H₈₄O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 180074-74-2
C₆₃H₈₀O₁₇

: 180074-75-3
C₇₀H₈₄O₁₇

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; for 1h; Ambient temperature;
DOI:10.1016/0960-894X(96)00240-5

Reference yield:

: 34957-73-8
methyl 9-hydroxynonanoate

: 180074-75-3
C₇₀H₈₄O₁₇

Guidance literature:: Multi-step reaction with 11 steps

1: 80 percent / Ag₂O, AgOTf / CH₂Cl₂

2: NaOMe / methanol

3: 85 percent / p-TsOH / acetonitrile

4: 70 percent / Drierite / CH₂Cl₂; pyridine / -50 °C

5: 72 percent / Ag₂O / CH₂Cl₂

6: NaOMe / methanol

7: 82 percent / CuBr₂, TEABr, mol. sieve / dimethylformamide; CH₂Cl₂

8: 70 percent / NaBH₃CN, HCl / tetrahydrofuran; diethyl ether

9: 67 percent / BF₃*Et₂O / diethyl ether; CH₂Cl₂ / -10 - 0 °C

10: NaOMe / methanol

11: 83 percent / p-TsOH / acetonitrile / 1 h / Ambient temperature

With hydrogenchloride; calcium sulfate; molecular sieve; boron trifluoride diethyl etherate; tetraethylammonium bromide; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; copper(ll) bromide; silver(l) oxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0960-894X(96)00240-5

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 180074-75-3
C₇₀H₈₄O₁₇

Guidance literature:: Multi-step reaction with 9 steps

1: 85 percent / p-TsOH / acetonitrile

2: 70 percent / Drierite / CH₂Cl₂; pyridine / -50 °C

3: 72 percent / Ag₂O / CH₂Cl₂

4: NaOMe / methanol

5: 82 percent / CuBr₂, TEABr, mol. sieve / dimethylformamide; CH₂Cl₂

6: 70 percent / NaBH₃CN, HCl / tetrahydrofuran; diethyl ether

7: 67 percent / BF₃*Et₂O / diethyl ether; CH₂Cl₂ / -10 - 0 °C

8: NaOMe / methanol

9: 83 percent / p-TsOH / acetonitrile / 1 h / Ambient temperature

With hydrogenchloride; calcium sulfate; molecular sieve; boron trifluoride diethyl etherate; tetraethylammonium bromide; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; copper(ll) bromide; silver(l) oxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0960-894X(96)00240-5