phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

Base Information

Chemical Name:phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside
CAS No.:1520094-81-8
Molecular Formula:C₂₃H₂₈O₁₁S
Molecular Weight:512.535
Hs Code.:

Synonyms:phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

Suppliers and Price of phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

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Technology Process of phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

There total 1 articles about phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 130404-54-5
1,2,3,4,6,7-Hexa-O-acetyl-L-glycero-α-D-manno-heptopyranose

: 108-98-5
thiophenol

: 1520094-81-8
phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

: 1520094-82-9
phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-β-D-mannoheptopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 23h; Inert atmosphere;
DOI:10.1021/jo402312x

Reference yield: 98.0%

: 1520094-81-8
phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

: 1520094-83-0
phenyl 1-thio-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 4h;
DOI:10.1021/jo402312x

Reference yield:

: 1520094-81-8
phenyl 2,3,4,6,7-penta-O-acetyl-1-thio-L-glycero-α-D-mannoheptopyranoside

: 1520094-85-2
2,3,4,6,7-penta-O-benzyl-L-glycero-D-manno-heptopyranose

: 1520094-86-3
2,3,4,6,7-penta-O-benzyl-L-glycero-D-manno-heptopyranose

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 4 h / 20 °C

2.1: sodium hydride / toluene; N,N-dimethyl-formamide / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: water; N-Bromosuccinimide / acetone / 0.33 h / -5 °C

With N-Bromosuccinimide; water; sodium methylate; sodium hydride; In methanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/jo402312x