C₄₀H₄₆F₂N₄O₆

Base Information

Chemical Name:C₄₀H₄₆F₂N₄O₆
CAS No.:1311411-93-4
Molecular Formula:C₄₀H₄₆F₂N₄O₆
Molecular Weight:716.825
Hs Code.:

C<sub>40</sub>H<sub>46</sub>F<sub>2</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:C₄₀H₄₆F₂N₄O₆

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Chemical Property of C₄₀H₄₆F₂N₄O₆

Chemical Property:

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Technology Process of C₄₀H₄₆F₂N₄O₆

There total 17 articles about C₄₀H₄₆F₂N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1311411-91-2
C₄₆H₆₀F₂N₄O₆Si

: 1311411-93-4
C₄₀H₄₆F₂N₄O₆

Guidance literature:: C₄₆H₆₀F₂N₄O₆Si; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 50 ℃;

With water; In tetrahydrofuran;

Reference yield:

: 27200-79-9
p-bromophenylacetaldehyde

: 1311411-93-4
C₄₀H₄₆F₂N₄O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: formic acid / water; methanol / 24 h / 40 °C

2.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.33 h / -78 °C

2.3: -40 °C

3.1: Chiralpak Daicel^.(R). AD-20 / isopropyl alcohol / Resolution of racemate

4.1: hydrogen / tetrahydrofuran / 3 h / 25 °C

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

5.2: 1.5 h / -78 °C

6.1: sodium hydroxide / water; methanol / 3 h / 20 °C

6.2: pH 2 - 3

7.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

8.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

9.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.83 h / 100 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 50 °C

With 1H-imidazole; n-butyllithium; formic acid; tetrabutyl ammonium fluoride; hydrogen; sodium carbonate; triethylamine; diisopropylamine; HATU; sodium hydroxide; lithium hexamethyldisilazane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 4654-39-1
4-bromophenethanol

: 1311411-93-4
C₄₀H₄₆F₂N₄O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydrogencarbonate; sodium hypochlorite; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 0 °C

2.1: formic acid / water; methanol / 24 h / 40 °C

3.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

3.2: 0.33 h / -78 °C

3.3: -40 °C

4.1: Chiralpak Daicel^.(R). AD-20 / isopropyl alcohol / Resolution of racemate

5.1: hydrogen / tetrahydrofuran / 3 h / 25 °C

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

6.2: 1.5 h / -78 °C

7.1: sodium hydroxide / water; methanol / 3 h / 20 °C

7.2: pH 2 - 3

8.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

9.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

10.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.83 h / 100 °C / Inert atmosphere

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 50 °C

With 1H-imidazole; sodium hypochlorite; n-butyllithium; formic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; hydrogen; sodium hydrogencarbonate; sodium carbonate; triethylamine; diisopropylamine; HATU; sodium bromide; sodium hydroxide; lithium hexamethyldisilazane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;