Technology Process of C20H31N3O4SSi
There total 1 articles about C20H31N3O4SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / ethanol / Reflux
2: methanesulfonic acid
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 50 - 100 °C
4: 3-chloro-benzenecarboperoxoic acid / dichloromethane
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; methanesulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
1,4-dioxane; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.06.021
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetraethylammonium fluoride / acetonitrile
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1,4-dioxane / 50 - 100 °C
3: acetonitrile / Reflux
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetraethylammonium fluoride; triethylamine;
In
1,4-dioxane; acetonitrile;
2: Sonogashira coupling;
DOI:10.1016/j.bmcl.2012.06.021
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetraethylammonium fluoride / acetonitrile
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1,4-dioxane / 50 - 100 °C
3: acetonitrile / Reflux
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetraethylammonium fluoride; triethylamine;
In
1,4-dioxane; acetonitrile;
2: Sonogashira coupling;
DOI:10.1016/j.bmcl.2012.06.021