2-hydroxy-5-nitro diphenylsulphone

Base Information

• Chemical Name: 2-hydroxy-5-nitro diphenylsulphone
• CAS No.: 103858-78-2
• Molecular Formula: C₁₂H₉NO₅S
• Molecular Weight: 279.273
• Mol file: 103858-78-2.mol

Synonyms:2-hydroxy-5-nitro diphenylsulphone

Chemical Property of 2-hydroxy-5-nitro diphenylsulphone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-hydroxy-5-nitro diphenylsulphone

There total 2 articles about 2-hydroxy-5-nitro diphenylsulphone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

3-nitro-(phenylsulfonyl)benzene (18513-19-4) → 2-nitro-4-phenylsulfonylphenol (2493-66-5) + 2-hydroxy-5-nitro diphenylsulphone (103858-78-2)

Guidance literature:

With Cumene hydroperoxide; potassium tert-butylate; In N,N-dimethyl-formamide; at -5 - 5 ℃; for 2h;

DOI:10.1002/prac.19923340609

Reference yield:

4-chloro-1-nitro-3-phenylsulfonylbenzene (104094-47-5) → 2-hydroxy-5-nitro diphenylsulphone (103858-78-2)

Guidance literature:

With acetamide; sodium acetate;

Reference yield:

2-hydroxy-5-nitro diphenylsulphone (103858-78-2) → 2-phenylsulfonyl-4-aminophenol (84452-49-3)

Guidance literature:

With sodium dithionite;

upstream raw materials:

4-chloro-1-nitro-3-phenylsulfonylbenzene

3-nitro-(phenylsulfonyl)benzene

Downstream raw materials:

2-phenylsulfonyl-4-aminophenol