Technology Process of 3-(tert-butyldiphenylsilyloxy)-4-methylaniline
There total 3 articles about 3-(tert-butyldiphenylsilyloxy)-4-methylaniline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
dichloromethane;
at 20 ℃;
for 24h;
under 3750.38 Torr;
DOI:10.1055/s-0035-1560359
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 0.17 h / 20 °C
1.2: 4 h / 20 °C
2.1: palladium 10% on activated carbon; hydrogen / dichloromethane / 24 h / 20 °C / 3750.38 Torr
With
1H-imidazole; palladium 10% on activated carbon; hydrogen;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0035-1560359
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1H-imidazole / dichloromethane / 5 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 20 °C
With
1H-imidazole; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; dichloromethane;
DOI:10.1080/10286020.2017.1327952
