5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole

Base Information

• Chemical Name: 5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole
• CAS No.: 96540-16-8
• Molecular Formula: C₂₈H₂₄O₆S₂
• Molecular Weight: 520.627

Synonyms:5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole

Chemical Property of 5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole

Chemical Property:

Purity/Quality:

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Technology Process of 5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole

There total 2 articles about 5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-(N-morpholino)cyclopent-1-ene (936-52-7) → 5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole (96540-16-8)

Guidance literature:

In tetrahydrofuran; Heating;

DOI:10.1016/S0040-4039(00)98468-5

Reference yield: 74.0%

cyclopentanone (120-92-3) → 5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole (96540-16-8)

Guidance literature:

With morpholine; toluene-4-sulfonic acid; In benzene; for 5h; Heating; Dean-Stark apparatus;

DOI:10.1016/S0040-4039(00)98468-5

Reference yield:

5-(5,7-Bis-benzenesulfonyl-2,3,3a,4-tetrahydro-1H-inden-4-yl)-benzo[1,3]dioxole (96540-16-8) → 5-(5,7-Bis-benzenesulfonyl-indan-4-yl)-benzo[1,3]dioxole (96540-22-6)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; Yield given; Heating;

DOI:10.1016/S0040-4039(00)98468-5

upstream raw materials:

1-(N-morpholino)cyclopent-1-ene

cyclopentanone

Downstream raw materials:

5-(5,7-Bis-benzenesulfonyl-indan-4-yl)-benzo[1,3]dioxole

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