ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁

Base Information

Chemical Name:ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁
CAS No.:675882-39-0
Molecular Formula:C₁₈H₂₄Cl₂SiZr
Molecular Weight:430.604
Hs Code.:

ZrCl<sub>2</sub>Si(CH<sub>3</sub>)2C<sub>5</sub>H<sub>4</sub>C<sub>5</sub>H<sub>3</sub>C<sub>6</sub>H<sub>11</sub>

Synonyms:ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁

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Chemical Property of ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁

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Technology Process of ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁

There total 1 articles about ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 21959-01-3,125410-70-0,125410-71-1
zirconium tetrachloride bis(tetrahydrofuran) complex

: 2Li⁽¹⁺⁾*Si(CH₃)2C₅H₄C₅H₃C₆H₁₁^(2-)=Li₂(Si(CH₃)2C₅H₄C₅H₃C₆H₁₁)

: 675882-39-0
ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁

Guidance literature:: In toluene; ligand and Zr-complex were mixed in Schlenk flask, cooled to -78°C, toluene was added, warmed to room temp., stirred overnight under Ar; vol. was reduced, stored at -20°C, collected, dried in vacuo; elem. anal.;
DOI:10.1021/ja035739y

Reference yield: 67.0%

: 675882-39-0
ZrCl₂Si(CH₃)2C₅H₄C₅H₃C₆H₁₁

: 917-54-4
methyllithium

: 675882-42-5
Zr(CH₃)2Si(CH₃)2C₅H₄C₅H₃C₆H₁₁

Guidance literature:: In diethyl ether; soln. of MeLi in ether was added dropwise to soln. of Zr-complex in toluene at -78°C, warmed to room temp. after 30 min, stirred for 2 h under Ar, toluene was added; filtered, washed with toluene, solvent was removed in vacuo, stirred in pentane at -78°C, filtered, dried in vacuo; elem. anal.;
DOI:10.1021/ja035739y