Technology Process of D-1,3,6-tri-O-benzoyl-myo-inositol 2,4,5-tris(diethyl phosphate)
There total 9 articles about D-1,3,6-tri-O-benzoyl-myo-inositol 2,4,5-tris(diethyl phosphate) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: TSA / dimethylformamide / 18 h / 20 °C
2: 349 mg / aqueous AcOH / dimethylformamide / 2 h / 20 °C
3: N,N-diisopropylethylamine / dimethylformamide / 12 h / -42 - 20 °C
4: sodium phosphate buffer; H2O2 / dimethylformamide
With
sodium phosphate buffer; dihydrogen peroxide; acetic acid; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
DOI:10.1021/jo0257694
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / aqueous AcOH / 3 h / 100 °C
2: TSA / dimethylformamide / 18 h / 20 °C
3: 349 mg / aqueous AcOH / dimethylformamide / 2 h / 20 °C
4: N,N-diisopropylethylamine / dimethylformamide / 12 h / -42 - 20 °C
5: sodium phosphate buffer; H2O2 / dimethylformamide
With
sodium phosphate buffer; dihydrogen peroxide; acetic acid; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
DOI:10.1021/jo0257694
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / aqueous AcOH / 3 h / 100 °C
2: TSA / dimethylformamide / 18 h / 20 °C
3: 349 mg / aqueous AcOH / dimethylformamide / 2 h / 20 °C
4: N,N-diisopropylethylamine / dimethylformamide / 12 h / -42 - 20 °C
5: sodium phosphate buffer; H2O2 / dimethylformamide
With
sodium phosphate buffer; dihydrogen peroxide; acetic acid; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
DOI:10.1021/jo0257694
