9-triptycene phenethyl selenoxide

Base Information

Chemical Name:9-triptycene phenethyl selenoxide
CAS No.:1534328-09-0
Molecular Formula:C₂₈H₂₂OSe
Molecular Weight:453.442
Hs Code.:

Synonyms:9-triptycene phenethyl selenoxide

Suppliers and Price of 9-triptycene phenethyl selenoxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-triptycene phenethyl selenoxide

Chemical Property:

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Technology Process of 9-triptycene phenethyl selenoxide

There total 2 articles about 9-triptycene phenethyl selenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1534328-08-9
9-Triptycene Phenethyl Selenide

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1534328-09-0
9-triptycene phenethyl selenoxide

: 220918-01-4
9-triptyceneselenenic acid

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃;
DOI:10.1021/ja411493t

Reference yield:

: 103-63-9
1-phenyl-2-bromoethane

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1534328-09-0
9-triptycene phenethyl selenoxide

Guidance literature:: Multi-step reaction with 3 steps

1: selenium; sodium; naphthalene / tetrahydrofuran / 1 h / Inert atmosphere

2: n-butyllithium / benzene; tert-butyl methyl ether / 12 h / -78 - 20 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

With selenium; n-butyllithium; naphthalene; sodium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; tert-butyl methyl ether; benzene;
DOI:10.1021/ja411493t