C₃₁H₄₁N₃Si

Base Information

• Chemical Name: C₃₁H₄₁N₃Si
• CAS No.: 1361603-38-4
• Molecular Formula: C₃₁H₄₁N₃Si
• Molecular Weight: 483.772
• Mol file: 1361603-38-4.mol

Synonyms:C₃₁H₄₁N₃Si

Chemical Property of C₃₁H₄₁N₃Si

Chemical Property:

Purity/Quality:

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Technology Process of C₃₁H₄₁N₃Si

There total 1 articles about C₃₁H₄₁N₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C21H34BrN3Si (1207685-27-5) + 1-Naphthylboronic acid (13922-41-3) → C31H41N3Si (1361603-38-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; toluene; for 24h; Inert atmosphere; Reflux;

DOI:10.1002/chem.201103133

Reference yield: 96.0%

C31H41N3Si (1361603-38-4) → C27H31ISi (1361603-42-0)

Guidance literature:

With methyl iodide; at 120 ℃; for 22h;

DOI:10.1002/chem.201103133

Reference yield:

C31H41N3Si (1361603-38-4) → C18H11I

Guidance literature:

Multi-step reaction with 2 steps

1: methyl iodide / 22 h / 120 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

With tetrabutyl ammonium fluoride; methyl iodide; In tetrahydrofuran;

DOI:10.1002/chem.201103133

upstream raw materials:

C₂₁H₃₄BrN₃Si

1-Naphthylboronic acid

Downstream raw materials:

C₂₇H₃₁ISi