O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate

Base Information

Chemical Name:O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate
CAS No.:472966-59-9
Molecular Formula:C₂₈H₂₇N₂O₄P
Molecular Weight:486.507
Hs Code.:

Synonyms:O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate

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Chemical Property of O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate

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Technology Process of O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate

There total 6 articles about O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 100-46-9
benzylamine

: C₂₁H₁₉ClNO₄P

: 472966-59-9
O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate

Guidance literature:: With triethylamine; In chloroform; at 20 ℃;
DOI:10.1016/S0040-4020(02)00561-6

Reference yield:

: 101-02-0
triphenyl phosphite

: 472966-59-9
O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / AcOH

2: 86 percent / NaOH; 18-crown-6; potassium fluoride / dioxane / pH 1

3: SOCl₂ / benzene / 2 h / Heating

4: 61 percent / triethylamine / CHCl₃ / 20 °C

With potassium fluoride; sodium hydroxide; thionyl chloride; 18-crown-6 ether; acetic acid; triethylamine; In 1,4-dioxane; chloroform; benzene;
DOI:10.1016/S0040-4020(02)00561-6

Reference yield:

: 621-84-1
O-benzyl carbamate

: 472966-59-9
O-phenyl N-benzyl-P-[{[(benzyloxy)carbonyl]amino}(phenyl)methyl]phosphonamidate

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / AcOH

2: 86 percent / NaOH; 18-crown-6; potassium fluoride / dioxane / pH 1

3: SOCl₂ / benzene / 2 h / Heating

4: 61 percent / triethylamine / CHCl₃ / 20 °C

With potassium fluoride; sodium hydroxide; thionyl chloride; 18-crown-6 ether; acetic acid; triethylamine; In 1,4-dioxane; chloroform; benzene;
DOI:10.1016/S0040-4020(02)00561-6