(2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal

Base Information

• Chemical Name: (2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal
• CAS No.: 223907-63-9
• Molecular Formula: C₃₃H₄₆O₄Si
• Molecular Weight: 534.811

Synonyms:(2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal

Chemical Property of (2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal

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Technology Process of (2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal

There total 2 articles about (2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[4-(tert-butyl-dimethyl-silanyloxy)-but-1-enyl]-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-8-[1,3]dioxolan-2-yl-4-methyl-non-7-en-2-one → (2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal (223907-63-9)

Guidance literature:

With acetic acid; In tetrahydrofuran; water; Yield given; Ambient temperature;

DOI:10.1016/S0040-4039(99)00187-2

Reference yield:

(E)-4-[(E)-4-(tert-Butyl-dimethyl-silanyloxy)-but-1-enyl]-8-[1,3]dioxolan-2-yl-3-(2-hydroxy-ethyl)-4-methyl-non-7-en-2-one (188568-15-2) → (2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal (223907-63-9)

Guidance literature:

Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / Ambient temperature

2: AcOH / tetrahydrofuran; H₂O / Ambient temperature

With 1H-imidazole; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(99)00187-2

Reference yield: 99.0%

p-toluenesulfonyl chloride (98-59-9) + (2E,7E)-6-{1-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-10-hydroxy-2,6-dimethyl-deca-2,7-dienal (223907-63-9) → Toluene-4-sulfonic acid (3E,8E)-5-{1-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2-oxo-propyl}-5,9-dimethyl-10-oxo-deca-3,8-dienyl ester

Guidance literature:

With pyridine; In chloroform;

DOI:10.1016/S0040-4039(99)00187-2

upstream raw materials:

(E)-4-[(E)-4-(tert-Butyl-dimethyl-silanyloxy)-but-1-enyl]-8-[1,3]dioxolan-2-yl-3-(2-hydroxy-ethyl)-4-methyl-non-7-en-2-one

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