5-methyl-5'-nitro-BAPTA tetramethyl ester

Base Information

• Chemical Name: 5-methyl-5'-nitro-BAPTA tetramethyl ester
• CAS No.: 1329676-52-9
• Molecular Formula: C₂₇H₃₃N₃O₁₂
• Molecular Weight: 591.572

Synonyms:5-methyl-5'-nitro-BAPTA tetramethyl ester

Chemical Property of 5-methyl-5'-nitro-BAPTA tetramethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 5-methyl-5'-nitro-BAPTA tetramethyl ester

There total 1 articles about 5-methyl-5'-nitro-BAPTA tetramethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

N-(2-(2-(2-(bis(methoxycarbonylmethyl)amino)phenoxy)ethoxy)-4-methylphenyl)-N-(methoxycarbonylmethyl)aminoacetic acid methyl ester (96315-10-5) → 5-methyl-5'-nitro-BAPTA tetramethyl ester (1329676-52-9)

Guidance literature:

With sulfuric acid; nitric acid; acetic acid; at 100 ℃; for 0.05h;

Reference yield: 72.0%

5-methyl-5'-nitro-BAPTA tetramethyl ester (1329676-52-9) → 5-methyl-5'-nitro BAPTA

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 14h;

Reference yield: 47.0%

5-methyl-5'-nitro-BAPTA tetramethyl ester (1329676-52-9) → 5-amino-5′-methyl BAPTA tetramethyl ester (1329676-54-1)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 2h;

DOI:10.1021/ja205809h

upstream raw materials:

N-(2-(2-(2-(bis(methoxycarbonylmethyl)amino)phenoxy)ethoxy)-4-methylphenyl)-N-(methoxycarbonylmethyl)aminoacetic acid methyl ester

Downstream raw materials:

5-amino-5′-methyl BAPTA tetramethyl ester

C₅₀H₅₆N₅O₁₁Si⁽¹⁺⁾

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