N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide

Base Information

Chemical Name:N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide
CAS No.:1417620-40-6
Molecular Formula:C₂₁H₂₀ClN₃O₄
Molecular Weight:413.861
Hs Code.:

Synonyms:N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide

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Chemical Property of N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide

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Technology Process of N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide

There total 2 articles about N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2-(4-chlorophenyl)acetamidine hydrochloride

: 1315456-69-9
2-(4-methoxy-3,5-dimethyl-benzoylamino)-malonic acid diethyl ester

: 1417620-40-6
N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide

Guidance literature:: 2-(4-chlorophenyl)acetamidine hydrochloride; With sodium methylate; In ethanol; for 0.25h;

2-(4-methoxy-3,5-dimethyl-benzoylamino)-malonic acid diethyl ester; In ethanol; at 80 ℃; for 2h;

Reference yield:

: 21668-34-8
3,5-dimethyl-4-methoxybenzoic acid chloride

: 1417620-40-6
N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 2 h / 0 °C

2.1: sodium methylate / ethanol / 0.25 h

2.2: 2 h / 80 °C

With sodium methylate; triethylamine; In ethanol; dichloromethane;