[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]⁽¹⁺⁾*AlCl₂(CH₃)2^(1-)=[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]AlCl₂(CH₃)2

Base Information

• Chemical Name: [W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]⁽¹⁺⁾*AlCl₂(CH₃)2^(1-)=[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]AlCl₂(CH₃)2
• CAS No.: 83634-39-3
• Molecular Formula: C₂H₆AlCl₂*C₁₈H₃₆NP₂W
• Molecular Weight: 640.245

Synonyms:[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]⁽¹⁺⁾*AlCl₂(CH₃)2^(1-)=[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]AlCl₂(CH₃)2

Chemical Property of [W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]⁽¹⁺⁾*AlCl₂(CH₃)2^(1-)=[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]AlCl₂(CH₃)2

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Technology Process of [W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]⁽¹⁺⁾*AlCl₂(CH₃)2^(1-)=[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]AlCl₂(CH₃)2

There total 1 articles about [W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]⁽¹⁺⁾*AlCl₂(CH₃)2^(1-)=[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2CH₃]AlCl₂(CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl2 (83634-33-7) + trimethylaluminum (75-24-1) → [W(NC6H5)(CHC(CH3)3)(P(CH3)3)2CH3](1+)*AlCl2(CH3)2(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2CH3]AlCl2(CH3)2 (83634-39-3)

Guidance literature:

In toluene; pentane; Al(CH3)3 added to stirred toluene-pentane soln. of W complex under N2; cooling to -30°C, filtration, washing with toluene and pentane; elem. anal.;

DOI:10.1021/ja00390a016

Reference yield: 91.0%

[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2CH3](1+)*AlCl2(CH3)2(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2CH3]AlCl2(CH3)2 (83634-39-3) → W(NC6H5)(CC(CH3)3)(Al(CH3)2Cl)(P(CH3)3)2Cl (83649-38-1)

Guidance literature:

In toluene; W complex suspd. in toluene, mixture heated at 50°C for 14 h under N2; filtration, concg. in vac., cooling to -30°C, concg., addn. of pentane, cooling to -30°C; elem. anal.;

DOI:10.1021/ja00390a016

upstream raw materials:

W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

trimethylaluminum

Downstream raw materials:

W(NC₆H₅)(CC(CH₃)3)(Al(CH₃)2Cl)(P(CH₃)3)2Cl

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