(1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine

Base Information

Chemical Name:(1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine
CAS No.:98245-07-9
Molecular Formula:C₃₀H₃₆N₄
Molecular Weight:452.643
Hs Code.:

Synonyms:(1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine

Chemical Property:

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Technology Process of (1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine

There total 10 articles about (1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2719-30-4
o-nitrophenylisothiocyanate

: 98245-07-9
(1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 25 °C

2: H₂, NH₃ / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

3: yellow HgO, sulfur / ethanol / 2 h / Heating

4: 48 percent aq. HBr / 2 h / 120 °C

5: Na₂CO₃ / dimethylformamide / 70 °C

6: 1.) sodium hydride / 1.) dimethyl sulfoxide, benzene, 30 min, 2.) dimethyl sulfoxide, benzene, RT, overnight

With ammonia; hydrogen bromide; hydrogen; sodium hydride; sodium carbonate; sulfur; mercury(II) oxide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00150a029

Reference yield:

: 4-Propylamino-piperidine-1-carboxylic acid ethyl ester

: 98245-07-9
(1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 25 °C

2: H₂, NH₃ / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

3: yellow HgO, sulfur / ethanol / 2 h / Heating

4: 48 percent aq. HBr / 2 h / 120 °C

5: Na₂CO₃ / dimethylformamide / 70 °C

6: 1.) sodium hydride / 1.) dimethyl sulfoxide, benzene, 30 min, 2.) dimethyl sulfoxide, benzene, RT, overnight

With ammonia; hydrogen bromide; hydrogen; sodium hydride; sodium carbonate; sulfur; mercury(II) oxide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00150a029

Reference yield:

: 75971-34-5
(1-Phenethyl-piperidin-4-yl)-propyl-amine

: 98245-07-9
(1-Benzyl-1H-benzoimidazol-2-yl)-(1-phenethyl-piperidin-4-yl)-propyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 25 °C

2: H₂, NH₃ / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

3: yellow HgO, sulfur / ethanol / 2 h / Heating

4: 1.) sodium hydride / 1.) dimethyl sulfoxide, benzene, 30 min, 2.) dimethyl sulfoxide, benzene, RT, overnight

With ammonia; hydrogen; sodium hydride; sulfur; mercury(II) oxide; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00150a029