9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

Base Information

Chemical Name:9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine
CAS No.:1631755-15-1
Molecular Formula:C₄₂H₅₄N₂O₂
Molecular Weight:618.903
Hs Code.:

Synonyms:9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

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Chemical Property of 9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

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Technology Process of 9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

There total 4 articles about 9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.9%

: 30752-19-3
1-bromo-4-hexyloxylbenzene

: 1631755-60-6
C₃₀H₃₈N₂O

: 1631755-15-1
9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

Guidance literature:: With tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate; In 1,2-dimethoxyethane; Inert atmosphere; Reflux;
DOI:10.1021/ol5018036

Reference yield:

: 1631755-88-8
C₁₈H₁₉BrN₂O₂

: 1631755-15-1
9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

2: palladium on activated charcoal; hydrogen / tetrahydrofuran / 20 °C

3: palladium diacetate; tri-tert-butyl phosphine; potassium tert-butylate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium on activated charcoal; potassium tert-butylate; hydrogen; palladium diacetate; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; 1: |Suzuki Coupling;
DOI:10.1021/ol5018036

Reference yield:

: 921937-76-0
2-(4-(hexyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1631755-15-1
9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

2: palladium on activated charcoal; hydrogen / tetrahydrofuran / 20 °C

3: palladium diacetate; tri-tert-butyl phosphine; potassium tert-butylate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium on activated charcoal; potassium tert-butylate; hydrogen; palladium diacetate; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; 1: |Suzuki Coupling;
DOI:10.1021/ol5018036