3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid

Base Information

Chemical Name:3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid
CAS No.:726191-15-7
Molecular Formula:C₁₁H₁₂N₄O₅
Molecular Weight:280.24
Hs Code.:

Synonyms:3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid

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Chemical Property of 3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid

Chemical Property:

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Technology Process of 3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid

There total 5 articles about 3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 726191-14-6
N-(3-nitro-4-carboxyphenyl)-S-methylisothiourea

: 616-29-5
1,3-Diamino-2-hydroxypropane

: 726191-15-7
3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid

Guidance literature:: In ISOPROPYLAMIDE; at 80 ℃; for 18h;

Reference yield:

: HOOCC₆H₃NO₂NHCSNHCOC₆H₅

: 726191-15-7
3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methoxide / methanol / 1 h / 20 °C

2: ethanol / Heating

3: dimethylformamide / 100 °C

With sodium methylate; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2007.03.034

Reference yield:

: 618-84-8
3-amino-5-nitro-benzoic acid

: 726191-15-7
3-[N-(5-hydroxy-1,4,5,6-tetrahydropyrimidin-2-yl)amino]-5-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 1 h / 20 °C

2: sodium methoxide / methanol / 1 h / 20 °C

3: ethanol / Heating

4: dimethylformamide / 100 °C

With sodium methylate; In methanol; ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2007.03.034