3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate

Base Information

Chemical Name:3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate
CAS No.:1187056-60-5
Molecular Formula:C₂₄H₃₄O₆
Molecular Weight:418.53
Hs Code.:

Synonyms:3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate

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Chemical Property of 3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate

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Technology Process of 3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate

There total 7 articles about 3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₂O₅

: 108-24-7
acetic anhydride

: 1187056-60-5
3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate

Guidance literature:: With pyridine; dmap; at -78 - 0 ℃;
DOI:10.1016/j.tet.2009.06.035

Reference yield:

: 116780-31-5
(1R)-1-((4R,5S)-2,2-dimethyl-5-vinyl[1,3]dioxolan-4-yl)ethane-1,2-diol

: 1187056-60-5
3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; di(n-butyl)tin oxide; p-toluenesulfonyl chloride

2: magnesium; dilithium tetrachlorocuprate

3: dicyclohexyl-carbodiimide; dmap

4: diisobutylaluminium hydride

With dmap; dilithium tetrachlorocuprate; diisobutylaluminium hydride; di(n-butyl)tin oxide; magnesium; triethylamine; p-toluenesulfonyl chloride; dicyclohexyl-carbodiimide;
DOI:10.1055/s-0033-1340739

Reference yield:

: 50-69-1
D-ribose

: 1187056-60-5
3-(benzyloxy)-1-((R,Z)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)pent-3-enyloxy)propyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid

2: triethylamine; di(n-butyl)tin oxide; p-toluenesulfonyl chloride

3: magnesium; dilithium tetrachlorocuprate

4: dicyclohexyl-carbodiimide; dmap

5: diisobutylaluminium hydride

With dmap; dilithium tetrachlorocuprate; sulfuric acid; diisobutylaluminium hydride; di(n-butyl)tin oxide; magnesium; triethylamine; p-toluenesulfonyl chloride; dicyclohexyl-carbodiimide;
DOI:10.1055/s-0033-1340739