(S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester

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Chemical Name:(S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester
CAS No.:1329605-36-8
Molecular Formula:C₂₂H₂₉NO₆
Molecular Weight:403.475
Hs Code.:

Synonyms:(S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester

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Chemical Property of (S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester

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Technology Process of (S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester

There total 3 articles about (S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329166-58-6
2-bromo-1-(2-(but-3-enyloxy)phenyl)ethanone

: 90600-20-7
(2S)-2-[(tert-butoxycarbonyl)amino]pent-4-enoic acid

: 1329605-36-8
(S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester

Guidance literature:: (2S)-2-[(tert-butoxycarbonyl)amino]pent-4-enoic acid; With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

2-bromo-1-(2-(but-3-enyloxy)phenyl)ethanone; In N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 1329605-36-8
(S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / Reflux

2.1: copper(ll) bromide / ethyl acetate / 1 h / Reflux

3.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C

3.2: 0 - 20 °C

With potassium carbonate; potassium hydrogencarbonate; copper(ll) bromide; In ethyl acetate; N,N-dimethyl-formamide; acetone;

Reference yield:

: 108919-78-4
1-(2-(but-3-en-1-yloxy)phenyl)ethan-1-one

: 1329605-36-8
(S)-2-tert-butoxycarbonylamino-pent-4-enoic acid 2-(2-but-3-enyloxyphenyl)-2-oxo ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(ll) bromide / ethyl acetate / 1 h / Reflux

2.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C

2.2: 0 - 20 °C

With potassium hydrogencarbonate; copper(ll) bromide; In ethyl acetate; N,N-dimethyl-formamide;