C₂₉H₃₇NO₂Si

Base Information

Chemical Name:C₂₉H₃₇NO₂Si
CAS No.:1449383-37-2
Molecular Formula:C₂₉H₃₇NO₂Si
Molecular Weight:459.704
Hs Code.:

C<sub>29</sub>H<sub>37</sub>NO<sub>2</sub>Si

Synonyms:C₂₉H₃₇NO₂Si

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Chemical Property of C₂₉H₃₇NO₂Si

Chemical Property:

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Technology Process of C₂₉H₃₇NO₂Si

There total 15 articles about C₂₉H₃₇NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449383-36-1
C₂₆H₃₁NO₃Si

: 643021-30-1
1-phenyl-5-(propane-1-sulfonyl)-1H-1,2,3,4-tetrazole

: 1449383-37-2
C₂₉H₃₇NO₂Si

Guidance literature:: With potassium hexamethylsilazane; In 1,2-dimethoxyethane; toluene; at -55 - 20 ℃; for 2h;
DOI:10.1016/j.tet.2013.03.104

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1449383-37-2
C₂₉H₃₇NO₂Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: dmap; 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C

3.1: triethylamine; 4-acetamidobenzenesulfonyl azide / acetonitrile / 16 h / 20 °C

4.1: dichloromethane / 2 h / 0 - 20 °C

5.1: triethylamine / dichloromethane / 0 - 20 °C / Molecular sieve

5.2: 12 h / 20 °C

6.1: dirhodium tetraacetate / 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Reflux

7.1: sodium tetrahydroborate / methanol / 3 h / -30 - 20 °C

8.1: iodine; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C / Irradiation

9.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C

10.1: dicyclohexyl-carbodiimide / chloroform / 1 h / 20 °C / Irradiation

11.1: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 °C

12.1: potassium hexamethylsilazane / toluene; 1,2-dimethoxyethane / 2 h / -55 - 20 °C

With 1H-imidazole; dmap; dirhodium tetraacetate; sodium tetrahydroborate; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; 4-acetamidobenzenesulfonyl azide; hydrogen; iodine; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; hexane; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile; 8.1: |Suarez Lodo Functionalization / 10.1: |Barton Decarboxylation / 12.1: |Julia-Kocienski Olefination;
DOI:10.1016/j.tet.2013.03.104

Reference yield:

: methyl 2-[(6S)-6-ethenyl-2-oxo-1,3-oxazinan-4-yl]acetate

: 1449383-37-2
C₂₉H₃₇NO₂Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: triethylamine; dmap / dichloromethane / 20 °C

2.1: caesium carbonate / methanol / 24 h / 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

3.2: 2 h / 0 - 20 °C

3.3: 20 °C

4.1: 1H-imidazole / dichloromethane

5.1: dichloromethane / 2 h / 0 - 20 °C

6.1: triethylamine / dichloromethane / 0 - 20 °C / Molecular sieve

6.2: 12 h / 20 °C

7.1: dirhodium tetraacetate / 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Reflux

8.1: sodium tetrahydroborate / methanol / 3 h / -30 - 20 °C

9.1: iodine; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C / Irradiation

10.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C

11.1: dicyclohexyl-carbodiimide / chloroform / 1 h / 20 °C / Irradiation

12.1: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 °C

13.1: potassium hexamethylsilazane / toluene; 1,2-dimethoxyethane / 2 h / -55 - 20 °C

With 1H-imidazole; dmap; dirhodium tetraacetate; sodium tetrahydroborate; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; iodine; potassium hexamethylsilazane; diisobutylaluminium hydride; caesium carbonate; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; hexane; dichloromethane; chloroform; toluene; 9.1: |Suarez Lodo Functionalization / 11.1: |Barton Decarboxylation / 13.1: |Julia-Kocienski Olefination;
DOI:10.1016/j.tet.2013.03.104