C₂₀H₂₁NO₃

Base Information

Chemical Name:C₂₀H₂₁NO₃
CAS No.:1387007-02-4
Molecular Formula:C₂₀H₂₁NO₃
Molecular Weight:323.392
Hs Code.:

C<sub>20</sub>H<sub>21</sub>NO<sub>3</sub>

Synonyms:C₂₀H₂₁NO₃

Suppliers and Price of C₂₀H₂₁NO₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₀H₂₁NO₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₀H₂₁NO₃

There total 6 articles about C₂₀H₂₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1387007-01-3
C₂₀H₂₃NO₂

: 1387007-02-4
C₂₀H₂₁NO₃

Guidance literature:: With potassium permanganate; In water; tert-butyl alcohol; at 75 - 80 ℃; for 12h;
DOI:10.1016/j.tetasy.2012.05.012

Reference yield:

: 579-74-8
2-Methoxyacetophenone

: 1387007-02-4
C₂₀H₂₁NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: iodine / 3 h / 100 - 110 °C

2.1: sodium acetate; acetic acid / 100 - 110 °C / Inert atmosphere

2.2: 20 °C

3.1: boron tribromide / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

3.3: pH 7

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 3 h / 0 - 20 °C / Inert atmosphere

5.1: potassium permanganate / water; tert-butyl alcohol / 12 h / 75 - 80 °C

With potassium permanganate; iodine; sodium acetate; boron tribromide; sodium hydride; acetic acid; In tetrahydrofuran; dichloromethane; water; mineral oil; tert-butyl alcohol;
DOI:10.1016/j.tetasy.2012.05.012

Reference yield:

: 328242-20-2
(5S,7S)-(+)-5,6,7,8-tetrahydro-6,6-dimethyl-2-(2-hydroxyphenyl)-5,7-methanoquinoline

: 1387007-02-4
C₂₀H₂₁NO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 - 20 °C / Inert atmosphere

2.1: potassium permanganate / water; tert-butyl alcohol / 12 h / 75 - 80 °C

With potassium permanganate; sodium hydride; In tetrahydrofuran; water; mineral oil; tert-butyl alcohol;
DOI:10.1016/j.tetasy.2012.05.012