N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide

Base Information

Chemical Name:N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide
CAS No.:212835-44-4
Molecular Formula:C₁₅H₂₃NO₄S
Molecular Weight:313.418
Hs Code.:

Synonyms:N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide

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Chemical Property of N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide

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Technology Process of N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide

There total 4 articles about N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5332-66-1
Glycidyl m-nitrophenyl ether

: 212835-44-4
N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / 6 h / 80 °C

2: H₂ / 10percent Pd/C / ethanol / 8 h / Ambient temperature

3: Et₃N / CH₂Cl₂ / 3 h / 10 °C

With sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm970285z

Reference yield:

: 554-84-7
meta-nitrophenol

: 212835-44-4
N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) pyridine, 2.) aq. KOH / 1.) 90 deg C, 5 h, 2.) acetone, RT, 2 h

2: H₂SO₄ / 6 h / 80 °C

3: H₂ / 10percent Pd/C / ethanol / 8 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 3 h / 10 °C

With pyridine; potassium hydroxide; sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm970285z

Reference yield:

: 94925-79-8
1-Ethoxy-3-(3-nitro-phenoxy)-propan-2-ol

: 212835-44-4
N-[3-(3-Ethoxy-2-hydroxy-propoxy)-phenyl]-3-methylsulfanyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 8 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 3 h / 10 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm970285z