C₄₁H₅₆O₇SSi

Base Information

Chemical Name:C₄₁H₅₆O₇SSi
CAS No.:1334173-64-6
Molecular Formula:C₄₁H₅₆O₇SSi
Molecular Weight:721.043
Hs Code.:

C<sub>41</sub>H<sub>56</sub>O<sub>7</sub>SSi

Synonyms:C₄₁H₅₆O₇SSi

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Chemical Property of C₄₁H₅₆O₇SSi

Chemical Property:

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Technology Process of C₄₁H₅₆O₇SSi

There total 10 articles about C₄₁H₅₆O₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 20451-53-0
Phenyl vinyl sulfoxide

: 1334173-63-5
C₃₃H₄₈O₆Si

: 1334173-64-6
C₄₁H₅₆O₇SSi

Guidance literature:: C₃₃H₄₈O₆Si; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

Phenyl vinyl sulfoxide; With potassium fluoride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201103550

Reference yield:

: 1334173-57-7
C₂₅H₃₀O₃Si

: 1334173-64-6
C₄₁H₅₆O₇SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

1.2: 13 h / -78 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: dicobalt octacarbonyl / toluene / 1.5 h / 20 °C / Inert atmosphere

3.2: 12 h / 100 °C

4.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

5.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium borohydride; dicobalt octacarbonyl; borane-THF; tetra-(n-butyl)ammonium iodide; sodium hydride; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; toluene; mineral oil; 3.1: Pauson-Khand reaction / 3.2: Pauson-Khand reaction;
DOI:10.1002/anie.201103550

Reference yield:

: C₂₆H₃₄O₄Si

: 1334173-64-6
C₄₁H₅₆O₇SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridinium p-toluenesulfonate / isopropyl alcohol; toluene / 28 - 80 °C / Inert atmosphere

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2.2: 13 h / -78 °C / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: dicobalt octacarbonyl / toluene / 1.5 h / 20 °C / Inert atmosphere

4.2: 12 h / 100 °C

5.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

6.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

7.2: 0 - 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium borohydride; dicobalt octacarbonyl; borane-THF; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; isopropyl alcohol; toluene; mineral oil; 4.1: Pauson-Khand reaction / 4.2: Pauson-Khand reaction;
DOI:10.1002/anie.201103550