(cis-3-(benzyloxy)cyclohexyl)fluorodimethylstannane

Base Information

Chemical Name:(cis-3-(benzyloxy)cyclohexyl)fluorodimethylstannane
CAS No.:114737-83-6
Molecular Formula:C₁₅H₂₃FOSn
Molecular Weight:357.055
Hs Code.:

Synonyms:(cis-3-(benzyloxy)cyclohexyl)fluorodimethylstannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (cis-3-(benzyloxy)cyclohexyl)fluorodimethylstannane

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Technology Process of (cis-3-(benzyloxy)cyclohexyl)fluorodimethylstannane

There total 1 articles about (cis-3-(benzyloxy)cyclohexyl)fluorodimethylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 114737-81-4,114737-96-1
(cis-3-(benzyloxy)cyclohexyl)trimethylstannane

: 114737-83-6
(cis-3-(benzyloxy)cyclohexyl)fluorodimethylstannane

Guidance literature:: With NH₄F; BF₃*Et₂O; iodosylbenzene; In dichloromethane; under slight positive pressure of N2, addn. of BF3*Et2O to stirred suspn. of trimethylstannane compd. iodosylbenzene in CH2Cl2 at 0°C, yellow color developed, stirred for 30min at 0°C, addn. of aq. NH4F soln. stirred at 0°C for 1h; mixt. poured into water, extn. with CH2Cl2, dried, concd., flash-chromy. (CHCl3/MeOH); elem. anal.;
DOI:10.1021/ja00222a020