5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

Base Information

• Chemical Name: 5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin
• CAS No.: 90358-07-9
• Molecular Formula: C₇₅H₉₅N₈O₁₃PSi₃
• Molecular Weight: 1431.86

Synonyms:5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

Chemical Property of 5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

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Technology Process of 5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

There total 2 articles about 5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N4-Benzoyl-3'-O-(tert-butylsilyl)-5'-O-<(4-methoxyphenyl)(diphenyl)methyl>tubercidin (87119-58-2) → 5'-O-<(p-Anisyl)diphenylmethyl>-N4-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sym-collidine / tetrahydrofuran / 0.5 h / -78 °C

2: 2.) I₂/H₂O / 1.) THF, 1 h, -78 deg C; 1 h, room temp, 2.) THF/sym-collidine, 15 min room temp

With 2,4,6-trimethyl-pyridine; water; iodine; In tetrahydrofuran;

Reference yield:

Phosphorochloridous acid (2R,3R,4R,5R)-2-(4-benzoylamino-pyrrolo[2,3-d]pyrimidin-7-yl)-4-(tert-butyl-dimethyl-silanyloxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester methyl ester + N4-Benzoyl-2',3'-di-O-(tert-butyldimethylsilyl)tubercidin (87119-56-0) → 5'-O-<(p-Anisyl)diphenylmethyl>-N4-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-07-9)

Guidance literature:

With water; iodine; Yield given. Multistep reaction; 1.) THF, 1 h, -78 deg C; 1 h, room temp, 2.) THF/sym-collidine, 15 min room temp;

Reference yield: 77.0%

5'-O-<(p-Anisyl)diphenylmethyl>-N4-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-07-9) → N4-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90373-53-8)

Guidance literature:

With zinc dibromide; In methanol; nitromethane; for 0.0833333h;

upstream raw materials:

N⁴-Benzoyl-2',3'-di-O-(tert-butyldimethylsilyl)tubercidin

N⁴-Benzoyl-3'-O-(tert-butylsilyl)-5'-O-<(4-methoxyphenyl)(diphenyl)methyl>tubercidin

Downstream raw materials:

N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz

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