1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide

Base Information

• Chemical Name: 1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide
• CAS No.: 952570-01-3
• Molecular Formula: C₂₄H₃₅FIN₃O₄SSi
• Molecular Weight: 635.614

Synonyms:1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide

Chemical Property of 1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide

Chemical Property:

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Technology Process of 1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide

There total 1 articles about 1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[(2-tert-butyldimethylsilanyloxy)ethyl]-cyclopropanesulfonamide-N-(4-(2-fluoro-4-iodophenyl)-5,7-dimethyl)-1H-imidazo[4,5c]pyridine-2,6(3H,5H)-dione (952570-00-2) → 1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide (952570-01-3)

Guidance literature:

With potassium trimethylsilonate; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

1-[2-(tert-Butyldimethylsilanyloxy)ethyl]-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide (952570-01-3) → 1-(2-Hydroxyethyl)-N-(4-(2-fluoro-4-iodophenylamino)-1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)cyclopropanesulfonamide

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 20 ℃; for 1.25h;

upstream raw materials:

1-[(2-tert-butyldimethylsilanyloxy)ethyl]-cyclopropanesulfonamide-N-(4-(2-fluoro-4-iodophenyl)-5,7-dimethyl)-1H-imidazo[4,5c]pyridine-2,6(3H,5H)-dione

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