3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone

Base Information

• Chemical Name: 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone
• CAS No.: 1361026-58-5
• Molecular Formula: C₁₃H₁₃BrO₄
• Molecular Weight: 313.148

Synonyms:3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone

Chemical Property of 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone

Chemical Property:

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Technology Process of 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone

There total 6 articles about 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C20H19BrO4 (1361026-61-0) → 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone (1361026-58-5) + 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-L-glycero-D-ido-heptono-1,4-lactone (1361026-59-6)

Guidance literature:

With titanium(IV) bromide; In dichloromethane; at 0 - 20 ℃; for 5h;

DOI:10.1016/j.tetlet.2012.01.121

Reference yield: 53.0%

3,6-anhydro-7-O-benzoyl-5-O-benzyl-2-deoxy-7-C-phenyl-D-glycero-D-ido-heptono-1,4-lactone (1234573-87-5) → 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone (1361026-58-5) + 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-L-glycero-D-ido-heptono-1,4-lactone (1361026-59-6)

Guidance literature:

With titanium(IV) bromide; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1016/j.tetlet.2012.01.121

Reference yield: 50.0%

3,6-anhydro-7-O-benzoyl-5-O-benzyl-2-deoxy-7-C-phenyl-D-glycero-L-ido-heptono-1,4-lactone (1361026-56-3) → 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-D-glycero-D-ido-heptono-1,4-lactone (1361026-58-5) + 3,6-anhydro-2,7-dideoxy-7-C-phenyl-7-bromo-L-glycero-D-ido-heptono-1,4-lactone (1361026-59-6)

Guidance literature:

With titanium(IV) bromide; In dichloromethane; at 0 - 20 ℃; for 5h;

DOI:10.1016/j.tetlet.2012.01.121

upstream raw materials:

3,6-anhydro-7-O-benzoyl-5-O-benzyl-2-deoxy-7-C-phenyl-D-glycero-D-ido-heptono-1,4-lactone

C₂₀H₁₉BrO₄

C₂₀H₁₉BrO₄

3,6-anhydro-7-O-benzoyl-5-O-benzyl-2-deoxy-7-C-phenyl-D-glycero-L-ido-heptono-1,4-lactone

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