5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:243136-83-6
Molecular Formula:C₃₈H₄₈N₄O₁₅
Molecular Weight:800.817
Hs Code.:

Synonyms:5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about 5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: Acetic acid (2S,4aR,6S,7R,8S,8aS)-7-acetoxy-6-{(2R,3S,4R,5R,6R)-5-amino-6-[2-(2-azido-ethoxy)-ethoxy]-2-benzyloxymethyl-4-hydroxy-tetrahydro-pyran-3-yloxy}-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

: 243136-83-6
5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 24h;
DOI:10.1016/S0008-6215(99)00022-1

Reference yield: 94.0%

: 243136-83-6
5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 243136-84-7
5-azido-3-oxapentyl (2,3-di-O-acetyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With water; acetic acid; at 100 ℃;
DOI:10.1016/S0008-6215(99)00022-1

Reference yield:

: 243136-83-6
5-azido-3-oxapentyl (2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 5-azido-3-oxapentyl (methyl [5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-2-nonulopyranosyl]onate)-(2->6)-(2,3-di-O-acetyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / HOAc; water / 100 °C

2: 16.5 percent / 3A molecular sieves; N-iodosuccinimide; trifluoromethanesulfonic acid / acetonitrile / 4 h / -40 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; water; acetic acid; In acetonitrile; 1: Hydrolysis / 2: Etherification;
DOI:10.1016/S0008-6215(99)00022-1