6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester

Base Information

Chemical Name:6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester
CAS No.:1447810-94-7
Molecular Formula:C₂₅H₃₇BINO₅
Molecular Weight:569.288
Hs Code.:

Synonyms:6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester

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Chemical Property of 6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester

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Technology Process of 6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester

There total 7 articles about 6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 172264-25-4
(E)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-ol

: 344437-84-9
6-(2-iodobenzamido)hexanoic acid

: 1447810-94-7
6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester

Guidance literature:: (E)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-ol; 6-(2-iodobenzamido)hexanoic acid; With dmap; In dichloromethane; at 0 ℃;

With diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/c3ob41020j

Reference yield:

: 73448-13-2
tert-butyldimethylsilyl hex-5-yn-1-yl ether

: 1447810-94-7
6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 6 h / 75 °C

1.2: 1 h / 20 °C

2.1: dmap / dichloromethane / 0 °C

2.2: 12 h / 20 °C

With dmap; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob41020j

Reference yield:

: 928-90-5
5-hexyl-1-ol

: 1447810-94-7
6-(2-iodobenzamido)hexanoic acid 6(E)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)hex-5-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; dmap / dichloromethane / 26 h / 0 - 20 °C

2.1: tetrahydrofuran / 6 h / 75 °C

2.2: 1 h / 20 °C

3.1: dmap / dichloromethane / 0 °C

3.2: 12 h / 20 °C

With dmap; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob41020j