allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Base Information

Chemical Name:allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside
CAS No.:874904-96-8
Molecular Formula:C₄₃H₅₁NO₂₀
Molecular Weight:901.873
Hs Code.:

allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Synonyms:allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

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Chemical Property of allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

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Technology Process of allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

There total 3 articles about allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 154391-03-4
allyl 2,3-di-O-benzoyl-α-D-galactopyranoside

: 874904-90-2
methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-D-galacto-2-nonulopyranosonate 2-(N-phenyl)trifluoroacetimidate

: 874904-96-8
allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In benzene; at -78 ℃; for 6h; Molecular sieve;
DOI:10.1021/acs.joc.6b02106

Reference yield: 51.0%

: C₂₄H₃₈NO₁₆P

: 154391-03-4
allyl 2,3-di-O-benzoyl-α-D-galactopyranoside

: 874904-96-8
allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Guidance literature:: C₂₄H₃₈NO₁₆P; allyl 2,3-di-O-benzoyl-α-D-galactopyranoside; In tetrahydrofuran; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; Molecular sieve; Inert atmosphere;

Reference yield:

: 154391-03-4
allyl 2,3-di-O-benzoyl-α-D-galactopyranoside

: 874904-90-2
methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-D-galacto-2-nonulopyranosonate 2-(N-phenyl)trifluoroacetimidate

: C₄₃H₅₁NO₂₀

: 874904-96-8
allyl 2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In propiononitrile; at -78 ℃; for 1.01667h; optical yield given as %de; stereoselective reaction; Molecular sieve;
DOI:10.1039/c1ob06164j