1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine

Base Information

Chemical Name:1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine
CAS No.:936720-59-1
Molecular Formula:C₄₃H₇₁N₅O₁₀
Molecular Weight:818.064
Hs Code.:

Synonyms:1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine

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Chemical Property of 1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine

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Technology Process of 1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine

There total 3 articles about 1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 936720-58-0
1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-tetraethylenepentamine

: 24424-99-5
di-tert-butyl dicarbonate

: 936720-59-1
1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine

Guidance literature:: In methanol; at 20 ℃; for 24h;
DOI:10.1055/s-2007-965924

Reference yield:

: 1755-15-3
2-acetyldimedone

: 936720-59-1
1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / molecular sieves / ethanol / 24 h / 20 °C

2: 79 percent / methanol / 24 h / 20 °C

With molecular sieve; In methanol; ethanol;
DOI:10.1055/s-2007-965924

Reference yield:

: 112-57-2
N-(2-aminoethyl)-N'-{2-[(2-aminoethyl)amino]ethyl}ethane-1,2-diamine

: 936720-59-1
1,13-bis[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]-4,7,10-tris(Boc)tetraethylenepentamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / molecular sieves / ethanol / 24 h / 20 °C

2: 79 percent / methanol / 24 h / 20 °C

With molecular sieve; In methanol; ethanol;
DOI:10.1055/s-2007-965924