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C32H36NO12P

Base Information
  • Chemical Name:C32H36NO12P
  • CAS No.:92054-26-7
  • Molecular Formula:C32H36NO12P
  • Molecular Weight:657.611
  • Hs Code.:
C<sub>32</sub>H<sub>36</sub>NO<sub>12</sub>P

Synonyms:C32H36NO12P

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Chemical Property of C32H36NO12P
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Technology Process of C32H36NO12P

There total 7 articles about C32H36NO12P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In acetic acid; at 75 ℃; for 2h;
DOI:10.1021/ja00291a029
Guidance literature:
Multi-step reaction with 6 steps
1: 96 percent / 1,5-diazabicyclo<4.3.0>non-5-ene (DBN) / benzene / 1 h / 25 °C
2: toluene / 10 h / 90 °C
3: trifluoroacetic acid / CH2Cl2; methanol / 1 h
4: 90 percent / triethylamine (Et3N) / CH2Cl2 / 3.5 h / 0 °C
5: 2.) sodium hydride / 1.) benzene, 25 deg C, 20 h; 2.) THF, 25 deg C, 3 h
6: 77 percent / acetic acid / 2 h / 75 °C
With DBN; sodium hydride; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; acetic acid; toluene; benzene;
DOI:10.1021/ja00291a029
Guidance literature:
Multi-step reaction with 7 steps
1: 92 percent / N-bromosuccinimide (NBS), H2O, acetic acid / CH2Cl2 / 5 h / 25 °C
2: 96 percent / 1,5-diazabicyclo<4.3.0>non-5-ene (DBN) / benzene / 1 h / 25 °C
3: toluene / 10 h / 90 °C
4: trifluoroacetic acid / CH2Cl2; methanol / 1 h
5: 90 percent / triethylamine (Et3N) / CH2Cl2 / 3.5 h / 0 °C
6: 2.) sodium hydride / 1.) benzene, 25 deg C, 20 h; 2.) THF, 25 deg C, 3 h
7: 77 percent / acetic acid / 2 h / 75 °C
With N-Bromosuccinimide; DBN; water; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; acetic acid; toluene; benzene;
DOI:10.1021/ja00291a029
upstream raw materials:

C32H34NO11P

C30H29BrO9

C30H28O8

C30H28O9

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